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1 article(s) from Samantray, Sagarika

Design of a double-decker coordination cage revisited to make new cages and exemplify ligand isomerism

Sagarika Samantray,
Sreenivasulu Bandi and
Dillip K. Chand

Beilstein J. Org. Chem. 2019, 15, 1129–1140, doi:10.3762/bjoc.15.109

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Graphical Abstract

Figure 1: The ligands (i) L1 and (ii) L2 that are positional isomers (regioisomers).

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Scheme 1: (i)/(ii) Complexation of Pd(tmeda)(Y)₂ with the ligand L1 at 1:1 and 2:3 metal-to-ligand ratios, re...

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Figure 2: Partial ¹H NMR spectra in DMSO-d₆ for (i) L1, (ii) [Pd(tmeda)(L1)](NO₃)₂ (1a) and (iii) a mixture o...

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Figure 3: Partial ¹H NMR spectra in DMSO-d₆ for (i) L1, (ii) [Pd(L1)₂](NO₃)₂ (3a) and (iii) [(NO₃)₂@Pd₃(L1)₄]...

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Figure 4: Energy-minimized structures of (i) [Pd(tmeda)(L1)]²⁺, (ii) [Pd₃(tmeda)₃(L1)₂]⁶⁺, (iii) [Pd(L1)₂]²⁺,...

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Scheme 2: Reorganization of (i) a mixture of Pd(NO₃)₂ and 3a at a 2:1 ratio leading to 4a with a complete con...

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Scheme 3: Halide (F⁻, Cl⁻ and Br⁻ but not I⁻) encapsulation by the cavities of the double-decker cage.

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Figure 5: Partial ¹H NMR spectra at 400 MHz in DMSO-d₆ for (i) [(NO₃)₂@Pd₃(L1)₄](NO₃)₄ (4a), (ii) [(F)₂@Pd₃(L1...

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Published 21 May 2019

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